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6-Chloropicolinic acid

  • Cas number:4684-94-0
  • purity:99%
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Product Details

Quality manufacturer supply 6-Chloropicolinic acid 4684-94-0 in stock with high standard

  • Molecular Formula: C6H4ClNO2
  • Molecular Weight: 157.556
  • Appearance/Colour: Off-white plates 
  • Melting Point: 190-191°C 
  • Refractive Index: 1.5870 (estimate) 
  • Boiling Point: 323.2 °C at 760 mmHg 
  • PKA: 3.27±0.10(Predicted) 
  • Flash Point: 149.263 °C 
  • PSA: 50.19000 
  • Density: 1.47 g/cm3 
  • LogP: 1.43320 

6-Chloropicolinic acid(Cas 4684-94-0) Usage

InChI:InChI=1/C6H4ClNO2/c7-5-3-1-2-4(8-5)6(9)10/h1-3H,(H,9,10)

4684-94-0 Relevant articles

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Redemann et al.

, p. 207 (1964)

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Method for preparing aromatic carboxylic acid compound

-

Paragraph 0141-0143; 0162-0164; 0177, (2020/02/14)

The invention discloses a method for pre...

Method for preparing aldehyde and acid by electrochemical dehydrochlorination of polychloromethylpyridine derivatives

-

Paragraph 0035-0037; 0057-0060, (2020/08/27)

The invention discloses a method for pre...

Preparation method of 6-amino-2-picolinic acid

-

Paragraph 0028-0033, (2020/07/15)

The invention relates to the technical f...

Tandem one-pot CO2 reduction by PMHS and silyloxycarbonylation of aryl/vinyl halides to access carboxylic acids

Paridala, Kumaraswamy,Lu, Sheng-Mei,Wang, Meng-Meng,Li, Can

supporting information, p. 11574 - 11577 (2018/10/31)

The present study discloses the synthesi...

4684-94-0 Process route

2,6-dichloropyridine
2402-78-0

2,6-dichloropyridine

carbon dioxide
124-38-9,18923-20-1

carbon dioxide

6-chloropicolinic acid
4684-94-0

6-chloropicolinic acid

Conditions
Conditions Yield
carbon dioxide; With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate; In 1,4-dioxane; at 65 ℃; for 0.333333h; Schlenk technique;
2,6-dichloropyridine; With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; toluene; at 100 ℃; for 10h; Schlenk technique; Sealed tube;
45%
carbon dioxide; With o-phenylenebis(diphenylphosphine); copper(II) acetate monohydrate; In 1,4-dioxane; at 65 ℃; for 0.416667h; Schlenk technique;
2,6-dichloropyridine; With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; toluene; at 100 ℃; for 10h; Schlenk technique;
45%
nitrapyrin
1929-82-4

nitrapyrin

6-chloropicolinic acid
4684-94-0

6-chloropicolinic acid

Conditions
Conditions Yield
With sulfuric acid; water; at 100 ℃; for 8h;
90%
With sulfuric acid; at 100 ℃; for 6h; Time;
90%

4684-94-0 Upstream products

  • 18368-63-3
    18368-63-3

    6-chloro-2-picoline

  • 5140-72-7
    5140-72-7

    2-bromo-6-chloro-pyridine

  • 124-38-9
    124-38-9

    carbon dioxide

  • 2258-42-6
    2258-42-6

    formyl acetic anhydride

4684-94-0 Downstream products

  • 23628-31-1
    23628-31-1

    6-aminopicolinic acid

  • 6636-55-1
    6636-55-1

    methyl 6-chloropicolinate

  • 192699-04-0
    192699-04-0

    N,N'-bis[(6-chloropicolinyl)-L-Ser(t-Bu)-β-Ala]-1,4-phenylenediamine

  • 98-98-6
    98-98-6

    2-Picolinic acid

6-Chloropicolinic acid

CAS:4684-94-0

Purity:99%

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